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KMID : 1024520150240121569
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Journal of the Environmental Sciences
2015 Volume.24 No. 12 p.1569 ~ p.1582
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Development of Analytical Method and Monitoring of Organophosphorus Pesticides in the Raw Water and Clean Water by Liquid Chromatography-Tandem Mass Spectrometry
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Kim Kyung-A
Song Mi-Jung
Yeom Hoon-Sik
Son Hee-Jong
Lee Sang-Won
Choi Jin-Taek
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Abstract
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The analytical method for 16 organophosphorus pesticides was developed in this study. The 16 organophosphorus pesticides were analyzed by liquid chromatography-tandem mass spectrometry (LC/MS/MS) using on-line solid phase extraction (on-line SPE) with PLRP- S cartridge. Analysis of all analytes in the MS/MS was processed in the electrospray ioni-zation (ESI) positive mode. They are Azinphos ethyl, Chlorfenvinphos, Ethion, Famphur, Phosmet, Phosphamidon, Terbufos, Aspon, Chlorpyrifos-methyl, Crotoxyphos, Dichlofenthi-on, Dicrotophos, Fonofos, Thionazin, Dimethoate and Iprobenfos. Limits of detection (LODs) and Limits of quantification(LOQs) were obtained as 0.8~2.0 ng/L and 2.6~6.4 ng/L, respectively. All compounds were not detected at the 8 sampling points of the raw water and clean water.
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KEYWORD
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Organophosphorus pesticides, Liquid chromatography-tandem mass spectrometry, On-line solid phase extraction, Electrospray ionization, Azinphos ethyl
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